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Dec 23, 2015 · noticeable in 13C NMR spectra of alcohols in acetone-d 6, and distinct 13C NMR resonances are observed for carbons α- and β- to the alcohol moiety. 1H NMR spectra of alcohols in acetone-d 6 typically show an −OH resonance that has a lower integration due to partial incorporation of deuterium. Overlap Looking further at said solvents data sheet, I do see a significant change in the 13 C carbonyl resonances for acetic acid and TFA - it's ~ 179 ppm for acetic acid and ~ 164 ppm for TFA. That seems to be reasonable enough. People have been looking at deuterium exchange in small molecules and macromolecules via NMR for a while now.